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Iso whats wrong

Hey folks first time poster here ive been trying my hand at iso oil ... Im using 99% iso but when i finished my last batch it was hard (like it needs to be geated to get a pin in it) yet when i put a flame to it it cracles burns and produses a black flame im not sure what im doing wrong ... I feel ive evaporated it to much making it hard but it slike theres still alcohol causeing it to crackle any advice? ...method I make the wash in the freezer put the mixture in a pyrex dish put the dish...

Iso whats wrong

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